3-(Piperidin-1-ium-1-yl)-6-azoniaspiro­[5.5]undecane dibromide monohydrate
2011

Synthesis and Structure of a New Spiro Compound

publication Evidence: moderate

Author Information

Author(s): Gonzalez Jorge, Atilano-Coral Roberto, Peraza-Campos Ana Lilia, Ortegón-Reyna David, Álvarez Eleuterio

Primary Institution: Facultad de Ciencias Químicas, Campus Coquimatlán, Kilometro 9, Carretera Colima-Coquimatlán, Colima, CP 28400, Mexico

Hypothesis

The study investigates the synthesis and crystal structure of a new spiro compound derived from 4-piperidinopiperidine and dibromopentane.

Conclusion

The synthesized compound exhibits a unique crystal structure characterized by hydrogen bonding interactions.

Supporting Evidence

  • The compound was synthesized with a yield of 70%.
  • Crystals suitable for X-ray diffraction were obtained.
  • The crystal structure features hydrogen bonds between the compound and bromide ions.

Takeaway

The researchers made a new chemical compound by mixing two ingredients, and they found that it has a special structure with some parts sticking together like magnets.

Methodology

The compound was synthesized through a reaction of 4-piperidinopiperidine with dibromopentane, followed by crystallization and X-ray diffraction analysis.

Digital Object Identifier (DOI)

10.1107/S1600536811008713

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