Benzene-1,3,5-tricarb­oxy­lic acid–5-(pyridin-1-ium-3-yl)-5H-1,2,3,4-tetra­zol-5-ide (1/1)
2011

Crystal Structure of Benzene-1,3,5-tricarboxylic Acid and Pyridinium-Tetrazolate

publication Evidence: high

Author Information

Author(s): Meng Gao-Xiang, Ding Hao, Feng Ya-Min, Zhu Jian-Hui, Yang He-Lin

Primary Institution: Central China Normal University

Hypothesis

The study investigates the crystal structure of a compound formed from trimesic acid and pyridyl-tetrazole under hydrothermal conditions.

Conclusion

The crystal structure reveals a two-dimensional layer linked by various hydrogen bonds and π–π interactions, forming a three-dimensional network.

Supporting Evidence

  • The asymmetric unit consists of a neutral trimesic acid molecule and a zwitterionic pyridyl-tetrazolate.
  • The crystal structure features a two-dimensional layer stabilized by hydrogen bonds.
  • The layers are interconnected by π–π interactions between the aromatic rings.

Takeaway

Scientists made a special crystal by mixing certain chemicals and heating them up, and they found that the crystal has a unique structure with layers that stick together.

Methodology

The compound was synthesized under hydrothermal conditions and characterized using X-ray crystallography.

Digital Object Identifier (DOI)

10.1107/S1600536811021490

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