cis-Bis(2,2′-bipyridine-κ2N,N′)dichlorido­iron(III) perchlorate [FeCl2(C10H8N2)2]ClO4
2011

Crystal Structure of Iron(III) Complex with Bipyridine

publication Evidence: moderate

Author Information

Author(s): Zhi-Fang Zhang

Primary Institution: Yulin University

Hypothesis

The study aims to synthesize and report the crystal structure of a bipyridine iron(III) complex.

Conclusion

The crystal structure of the synthesized iron(III) complex shows a distorted octahedral geometry around the iron atom.

Supporting Evidence

  • The iron atom in the complex is coordinated by two bipyridine ligands and two chloride ions.
  • The bond lengths between iron and nitrogen are consistent with previous studies.
  • Weak hydrogen bonds and interactions help stabilize the crystal structure.

Takeaway

The researchers made a new type of iron complex using bipyridine, and they found that the shape of the complex is a bit squished, like a lopsided ball.

Methodology

The complex was synthesized by mixing bipyridine and sodium perchlorate with iron(III) chloride in methanol, followed by crystallization.

Limitations

The study primarily focuses on one specific iron(III) complex and does not explore other potential complexes.

Digital Object Identifier (DOI)

10.1107/S1600536811016035

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