Aqua­bis­(4-chloro-2-hy­droxy­benzoato-κO)(1,10-phenanthroline-κ2N,N′)zinc(II) [Zn(C7H4ClO3)2(C12H8N2)(H2O)]
2011

Crystal Structure of a Zinc Complex with Chlorine-Substituted Salicylate

publication Evidence: moderate

Author Information

Author(s): Nie Jing-Jing, Xu Xun, Xu Duan-Jun

Primary Institution: Zhejiang University, People’s Republic of China

Hypothesis

The study investigates the effect of chlorine-substitution on π-π stacking between benzene rings of chlorine-substituted salicylates.

Conclusion

The chlorine-substituted salicylate complex exhibits significant π-π stacking interactions between its aromatic rings.

Supporting Evidence

  • The Zn(II) cation is coordinated by two chloro-salicylate anions, one phenanthroline ligand, and one water molecule.
  • Significant π-π stacking interactions were observed between the aromatic rings of the chloro-salicylate anions.
  • The centroid-to-centroid distance between benzene rings indicates the presence of aromatic stacking.

Takeaway

This study looks at how adding chlorine to a chemical structure affects how its parts stack together, which is important for understanding how these chemicals behave.

Methodology

The compound was synthesized from an ethanol solution of 1,10-phenanthroline and an aqueous solution containing zinc nitrate, 4-chloro-salicylic acid, and sodium carbonate, followed by crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811020435

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