Tri-μ-oxido-bis­[(5,10,15,20-tetra­phenyl­porphyrinato-κ4N)niobium(V)] [Nb2(C44H28N4)2O3]
2011

Study of a Niobium Porphyrin Compound

publication Evidence: moderate

Author Information

Author(s): Soury Raoudha, Belkhiria Mohamed Salah, Daran Jean-Claude, Nasri Habib

Primary Institution: Université de Monastir, Tunisia

Conclusion

The study successfully characterized a dinuclear niobium(V) porphyrin complex with specific bond lengths and structural features.

Supporting Evidence

  • The niobium atoms in the compound are seven-coordinated.
  • The Nb—O bond lengths range from 1.757 to 2.331 Å.
  • The average niobium–pyrrole N atom distance is 2.239 Å.
  • The Nb⋯Nb separation is 2.8200 Å.
  • The dihedral angle between the two porphyrinate mean planes is 5.4°.

Takeaway

Scientists looked at a special niobium compound made with porphyrin, which is a type of molecule. They found out how the atoms are arranged and how far apart they are.

Methodology

The compound was synthesized and characterized using X-ray crystallography.

Digital Object Identifier (DOI)

10.1107/S1600536811020538

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