n-Tridecyl­amine chloride monohydrate C13H30N+·Cl−·H2O
2011

Crystal Structure of n-Tridecylamine Chloride Monohydrate

publication Evidence: moderate

Author Information

Author(s): Zhang Lijun, Di Youying, Dan Wenyan

Primary Institution: College of Chemistry and Chemical Engineering, Liaocheng University, Shandong, People’s Republic of China

Hypothesis

The study investigates the crystal structure of n-tridecylamine chloride monohydrate to understand its phase transition properties.

Conclusion

The crystal structure reveals that the alkyl chain is in an all-trans conformation and is stabilized by hydrogen bonds.

Supporting Evidence

  • The alkyl chain in the compound is in an all-trans conformation.
  • Hydrogen bonds connect the components into layers in the crystal structure.
  • Single crystals suitable for X-ray diffraction were prepared from the compound.

Takeaway

This study looks at a special chemical compound and how its parts fit together, which helps us understand how it might behave in different situations.

Methodology

The compound was prepared by adding hydrochloric acid to an ethanolic solution of n-tridecylamine, followed by heating and stirring under reflux, and single crystals were obtained through evaporation.

Digital Object Identifier (DOI)

10.1107/S1600536811006246

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