cis-Bis{1,1-dibenzyl-3-[(furan-2-yl)carbon­yl]thio­ureato-κ2 O,S}nickel(II) [Ni(C20H17N2O2S)2]
2011

Structure of a Nickel(II) Complex with Thio­urea Ligands

publication Evidence: high

Author Information

Author(s): Pérez Hiram, da Silva Cecilia C. P., Plutín Ana M., de Simone Carlos A., Ellena Javier

Primary Institution: Departamento de Química Inorgánica, Facultad de Química, Universidad de la Habana, Habana 10400, Cuba

Conclusion

The study reveals that the nickel(II) complex exhibits a distorted square-planar geometry with specific bond lengths and angles.

Supporting Evidence

  • The nickel atom is coordinated by sulfur and oxygen atoms from two thio­urea ligands.
  • The complex shows a dihedral angle of 20.33° between the chelating rings.
  • The bond lengths of Ni–S and Ni–O are consistent with related structures.

Takeaway

The researchers studied a nickel compound that is shaped like a square but is a bit twisted, showing how the atoms are connected.

Methodology

The compound was synthesized and characterized using X-ray crystallography.

Digital Object Identifier (DOI)

10.1107/S1600536811010749

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