Bis(N-nitroso-N-phenyl­hydroxy­laminato-κ2O,O′)(1,10-phenanthroline-κ2N,N′)lead(II) [Pb(C6H5N2O2)2(C12H8N2)]
2011

Lead(II) Complex with Cupferronate and 1,10-Phenanthroline

publication Evidence: high

Author Information

Author(s): Najafi Ezzatollah, Amini Mostafa M., Ng Seik Weng

Primary Institution: Shahid Beheshti University

Conclusion

The study presents the crystal structure of a lead(II) complex that exhibits a distorted penta­gonal bipyramidal geometry.

Supporting Evidence

  • The lead(II) complex was characterized using X-ray crystallography.
  • The geometry of the lead atom in the complex is a distorted penta­gonal bipyramid.
  • Two cupferronate ions and a 1,10-phenanthroline ligand coordinate to the lead atom.

Takeaway

Scientists made a special lead compound using two types of ligands, and they found that it has a unique shape.

Methodology

The compound was synthesized by mixing lead(II) nitrate with cupferron ligand and 1,10-phenanthroline in ethanol, followed by crystal growth.

Digital Object Identifier (DOI)

10.1107/S1600536811006787

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