Recovery and purification of acetic acid from extremely diluted solutions using a mixed bed ion exchange resin – technical feasibility
2025

Recovering Acetic Acid from Diluted Solutions

publication Evidence: high

Author Information

Author(s): Roncal Tomás, Aguirre Ainhoa, Belaustegui Yolanda, Andrés Elisabet

Primary Institution: TECNALIA, Basque Research and Technology Alliance (BRTA)

Hypothesis

Can a mixed bed ion exchange resin effectively recover and purify acetic acid from extremely diluted solutions?

Conclusion

The study demonstrates a successful method for recovering and purifying acetic acid from very diluted solutions, achieving high purity and concentration.

Supporting Evidence

  • The process achieved a recovery yield of 90.3% for acetic acid.
  • The final solution had a purity of 96.9% after purification.
  • Acetic acid concentration was increased by 15 times compared to the original solution.

Takeaway

This study shows how to clean and concentrate acetic acid from very weak solutions using special materials, making it easier to use in industries.

Methodology

The process involves demineralization followed by treatment with a mixed bed ion exchange resin and step-elution with sulfuric acid.

Limitations

The study primarily uses synthetic solutions, which may not fully represent real fermentation broths.

Digital Object Identifier (DOI)

10.1039/d4ra08341e

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