Redetermination of μ-oxido-bis­[bis­(N,N-diethyl­hydroxyl­aminato)­oxido­vanadium(V)] [V2(C4H10NO)4O3]
2011

Redetermination of a Vanadium Complex Structure

publication Evidence: high

Author Information

Author(s): Zhang Heng-Qiang, Jin Zhong-Min, Fan Xin, Zhang Qi-Ying

Primary Institution: East China Normal University

Hypothesis

The study aims to improve the precision of the geometric parameters of a vanadium complex compared to previous determinations.

Conclusion

The current study reports an improved precision of the derived geometric parameters of the vanadium complex.

Supporting Evidence

  • The study provides a detailed comparison of bond lengths and angles with previous determinations.
  • Improved precision in geometric parameters enhances the understanding of the compound's structure.

Takeaway

The researchers looked at a vanadium compound and found a more accurate way to describe its structure than was done before.

Methodology

The structure was determined using X-ray crystallography with a Bruker APEXII CCD diffractometer.

Limitations

The previous study did not deposit atomic coordinates or displacement parameters, which limited its accessibility.

Digital Object Identifier (DOI)

10.1107/S1600536811020551

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