2,2-Dimethyl-5-[(5-methyl­furan-2-yl)methyl­idene]-1,3-dioxane-4,6-dione
2011

Crystal Structure of a New Compound

publication Evidence: moderate

Author Information

Author(s): Wu-Lan Zeng

Primary Institution: Weifang University

Hypothesis

The study aims to synthesize and report the crystal structure of a new Meldrum's acid compound.

Conclusion

The crystal structure of the compound is stabilized by weak intermolecular hydrogen bonds.

Supporting Evidence

  • The asymmetric unit contains two independent molecules.
  • The 1,3-dioxane rings in each molecule are in envelope conformations.
  • The bond lengths and angles for the independent molecules agree well with each other.

Takeaway

The researchers made a new chemical compound and looked at its structure using special techniques to see how its atoms are arranged.

Methodology

The compound was synthesized using a mixture of malonic acid, acetic anhydride, and other reagents, followed by crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811002285

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