N-Benzoyl-N′-(1,10-phenanthrolin-5-yl)thio­urea dichloro­methane hemisolvate monohydrate
2011

Study of N-Benzoyl-N′-(1,10-phenanthrolin-5-yl)thio­urea

publication Evidence: moderate

Author Information

Author(s): Mat Rashid, Fatisha Liyana, Heng Lee Yook, Daran Jean-Claude, Kassim Mohammad B.

Primary Institution: Universiti Kebangsaan Malaysia

Conclusion

The study successfully characterized the crystal structure of N-Benzoyl-N′-(1,10-phenanthrolin-5-yl)thio­urea and its interactions.

Supporting Evidence

  • The title compound contains 1,10-phenanthroline and benzoyl fragments.
  • Molecules are linked by various types of hydrogen bonds.
  • Weak C—H⋯π and π–π stacking interactions were observed.
  • The study utilized the SQUEEZE procedure to handle disordered solvent molecules.

Takeaway

The researchers looked at a special chemical compound and found out how its molecules are arranged in a crystal.

Methodology

The compound was synthesized and its crystal structure was analyzed using X-ray diffraction.

Limitations

The modeling of the dichloromethane solvent molecule was challenging due to its disorder.

Digital Object Identifier (DOI)

10.1107/S160053681101734X

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