Synthesis and Phase Evolution of a Nanocrystalline FexCrNiAl (x = 1.0, 0.5, 0.25) High-Entropy Alloys by Mechanical Alloying
2024

Synthesis and Phase Evolution of High-Entropy Alloys

publication Evidence: high

Author Information

Author(s): Yang Danni, Liao Mingqing, Huang Jingtao, Han Tianyi, Qu Nan, Wang Yalin, Zhu Jingchuan

Primary Institution: Lanzhou University of Technology

Hypothesis

The study investigates the alloying behavior, morphology, and phase evolution of FexCrNiAl high-entropy alloys synthesized by mechanical alloying.

Conclusion

The nanocrystalline FexCrNiAl high-entropy alloy powders were successfully synthesized, showing a transformation from a supersaturated solid solution phase to equilibrium phases upon annealing.

Supporting Evidence

  • The powders achieved a crystalline size of ~80 nm after mechanical alloying.
  • The mean particle size of the alloyed powders was refined to 1.59 μm.
  • The phase transformation occurred during high-temperature annealing, leading to the formation of BCC and ordered BCC (B2) phases.

Takeaway

The researchers made special metal powders that are really tiny and strong, and they found out how these powders change when heated.

Methodology

The powders were synthesized using mechanical alloying followed by high-temperature annealing, and characterized using X-ray diffraction and scanning electron microscopy.

Digital Object Identifier (DOI)

10.3390/ma17246061

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