5,11,17,23,29-Penta-tert-butyl-31,32,33,34,35-penta­propoxycalix[5]arene dichloro­methane hemisolvate C70H100O5·0.5CH2Cl2
2011

Study of a New Calix[5]Arene Compound

publication Evidence: moderate

Author Information

Author(s): Pojarová Michaela, Dušek Michal, Budka Jan, Císařová Ivana, Makrlík Emanuel

Primary Institution: Institute of Physics, AS CR, v.v.i

Conclusion

The compound crystallizes as a solvate with specific molecular arrangements and interactions.

Supporting Evidence

  • The compound was prepared by alkylation of tert-butylcalix[5]arene.
  • Crystallization occurred from a mixture of dichloromethane and methanol.
  • The asymmetric unit contains two molecules of calix[5]arene and one molecule of dichloromethane.

Takeaway

Scientists created a new chemical compound and studied how its molecules are arranged in crystals.

Methodology

The compound was synthesized through alkylation and crystallized from a mixture of dichloromethane and methanol.

Digital Object Identifier (DOI)

10.1107/S1600536811000456

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