N,N′-Bis(2-chlorophenylsulfonyl)adipamide C18H18Cl2N2O6S2
2011
Structure of N,N-Bis(2-chlorophenylsulfonyl)adipamide
publication
Evidence: moderate
Author Information
Author(s): Rodrigues Vinola Z., Foro Sabine, Gowda B. Thimme
Primary Institution: Mangalore University
Hypothesis
The study investigates the structural characteristics of N,N-bis(2-chlorophenylsulfonyl)adipamide.
Conclusion
The structure of N,N-bis(2-chlorophenylsulfonyl)adipamide was successfully determined, revealing specific bond conformations and intermolecular hydrogen bonding.
Supporting Evidence
- The conformation of the N—H and C=O bonds in the compound is anti to each other.
- The dihedral angle between the planes of the benzene ring and the central part of the molecule is 89.6°.
- Intermolecular N—H⋯O(S) hydrogen bonds link the molecules into sheets along the b axis.
Takeaway
The researchers looked at a special chemical compound and found out how its parts are arranged and how they stick together.
Methodology
The compound was prepared through refluxing a mixture of adipic acid and 2-chlorobenzenesulfonamide, followed by characterization using infrared and NMR spectra.
Digital Object Identifier (DOI)
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