(1S,3R,8R)-9-(1-Amino­ethyl­idene)-2,2-dichloro-3,7,7-trimethyl­tricyclo­[6.4.0.01,3]undecan-10-one
2011

Synthesis and Structure of a New Compound from Cedar Oil

publication Evidence: high

Author Information

Author(s): Benharref Ahmed, Lassaba Essêdiya, Avignant Daniel, Oudahmane Abdelghani, Berraho Moha

Primary Institution: Laboratoire de Chimie Biomoléculaires, Substances Naturelles et Réactivité, URAC16, Faculté des Sciences, Semlalia, Marrakech, Morocco

Conclusion

The new compound was successfully synthesized and its structure was confirmed through X-ray crystallography.

Supporting Evidence

  • The compound was synthesized from β-himachalene isolated from Atlas cedar oil.
  • The structure was confirmed by NMR spectral analysis and single-crystal X-ray structure.
  • The molecule features a seven-membered ring fused to a five-membered ring.

Takeaway

Scientists made a new chemical from cedar oil and figured out what it looks like using special X-ray pictures.

Methodology

The compound was synthesized from β-himachalene and characterized using NMR and X-ray crystallography.

Digital Object Identifier (DOI)

10.1107/S1600536811005307

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