Organic Papers 2-Isopropyl-5-methyl­cyclo­hexyl cyclo­hex­yl(phen­yl)phosphinate C22H35O2P
2011

Study of a New Phosphinate Compound

publication Evidence: moderate

Author Information

Author(s): Xu Hao, Liu Li-Juan, Meng Fan-Jie, Zhao Chang-Qiu

Primary Institution: Liaocheng University, Shandong, People’s Republic of China

Hypothesis

What is the crystal structure of the compound 2-Isopropyl-5-methylcyclohexyl cyclohexyl(phenyl)phosphinate?

Conclusion

The compound exhibits a crystal structure with weak intermolecular hydrogen bonds linking the molecules.

Supporting Evidence

  • The compound was prepared through a reaction involving cyclohexyl magnesium chloride.
  • The crystal structure was analyzed using X-ray diffraction techniques.
  • Weak intermolecular hydrogen bonds were observed in the crystal structure.

Takeaway

The researchers made a new chemical compound and looked at how its molecules are arranged in a crystal.

Methodology

The compound was synthesized from O-menthyl phenylphosphoryl chloride and cyclohexyl magnesium chloride, followed by purification and crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811010592

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