[μ-1,4-Bis(1,2,4-triazol-1-ylmeth­yl)benzene]­bis­[aqua­(pyridine-2,6-dicarboxyl­ato)copper(II)] monohydrate [Cu2(C7H3NO4)2(C12H12N6)(H2O)2]·H2O
2011

Crystal Structure of a Copper Complex

publication Evidence: moderate

Author Information

Author(s): Dong Gui-Ying, He Cui-Hong, Tong-Fei Liu, Deng Xiao-Chen, Shi Xiao-Ge

Primary Institution: Hebei United University

Hypothesis

To understand the coordination behavior of the flexible ligand 1,4-bis(1,2,4-triazol-1-ylmethyl)benzene.

Conclusion

The compound exhibits a dinuclear structure with a distorted square-based pyramidal coordination geometry around the copper atom.

Supporting Evidence

  • The copper center is five-coordinated in a distorted square-based pyramidal coordination geometry.
  • The flexible ligand adopts a bis-monodentate bridging mode linking the copper atoms.
  • Strong hydrogen-bonding interactions stabilize the crystal structure.

Takeaway

Scientists studied a special copper compound to see how it holds together. They found that it has a unique shape that helps it stay stable.

Methodology

The compound was synthesized in a sealed reactor and analyzed using X-ray diffraction.

Digital Object Identifier (DOI)

10.1107/S1600536811022756

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