1-(3-Fluoro­phen­yl)-4,4,6-trimethyl-3,4-dihydro­pyrimidine-2(1H)-thione
2011

Study of a New Compound: 1-(3-Fluorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione

publication

Author Information

Author(s): Yamin Bohari M., Lawi Ruhana L., Salem Halima F.

Primary Institution: School of Chemical Sciences and Food Technology, Universiti Kebangsaan Malaysia

Conclusion

The compound exhibits a planar dihydropyrimidine ring and forms centrosymmetric dimers through hydrogen bonding.

Supporting Evidence

  • The dihydropyrimidine ring is essentially planar with a maximum deviation of 0.086 Å.
  • The benzene ring is almost perpendicular to the dihydropyrimidine ring with a dihedral angle of 83.97°.
  • The crystal packing is characterized by centrosymmetric dimers resulting from pairs of intermolecular N—H⋯S hydrogen bonds.

Takeaway

Scientists studied a new chemical compound that has a special structure and can form pairs with itself through bonds.

Methodology

The compound was synthesized using equimolar quantities of thiocyanic acid and 3-fluoroaniline in acetone, followed by crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811023671

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