[1,2-Bis­(diisopropyl­phosphan­yl)ethane-κ2 P,P′]dichloridonickel(II)–9H-carbazole (1/2) [NiCl2(C14H32P2)]·2C12H9N
2011

Study of a Nickel Complex with Carbazole

publication Evidence: moderate

Author Information

Author(s): Cañavera-Buelvas Farah, Flores-Alamo Marcos, García Juventino J.

Primary Institution: Facultad de Química, Universidad Nacional Autónoma de México

Conclusion

The nickel complex exhibits slight tetrahedral distortion from ideal square-planar geometry and shows potential for use in catalytic systems.

Supporting Evidence

  • The nickel complex shows slight tetrahedral distortion from ideal square-planar geometry.
  • Two symmetry-related 9H-carbazole molecules are present between adjacent nickel complexes.
  • The synthesis involves heating a mixture of nickel and carbazole in THF.

Takeaway

The researchers created a nickel compound that can help in making catalysts, which are substances that speed up chemical reactions.

Methodology

The compound was synthesized from a THF solution of [Ni(dppe)H]2 and 9H-carbazole, followed by crystallization from dichloromethane.

Digital Object Identifier (DOI)

10.1107/S1600536811010555

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