A Quantitative Chemometric Study of Pharmaceutical Tablet Formulations Using Multi-Spectroscopic Fibre Optic Probes
2024

Study of Pharmaceutical Tablet Formulations Using Fibre Optic Probes

Sample size: 16 publication 10 minutes Evidence: moderate

Author Information

Author(s): Remoto Peter J. G., Gordon Keith C., Fraser-Miller Sara J.

Primary Institution: University of Otago

Hypothesis

Can custom-designed fibre optic probes effectively analyze pharmaceutical tablet formulations using Raman and near-infrared spectroscopy?

Conclusion

The study demonstrated that different probe configurations could reliably collect data and showed robust quantitative performances.

Supporting Evidence

  • Probe A effectively estimated hydroxymethyl cellulose and lactose monohydrate content using near-infrared spectroscopy.
  • Probe B was most effective for estimating titanium dioxide content using a combination of Raman and near-infrared spectroscopy.
  • Indomethacin content was best estimated using a low-level fused dataset collected with spatially offset Raman spectroscopy.

Takeaway

Researchers created special tools to look inside medicine tablets without breaking them, helping to understand their ingredients better.

Methodology

The study used Raman and near-infrared spectroscopy to analyze pharmaceutical tablets, employing principal component analysis and partial least squares regression for data evaluation.

Limitations

The effectiveness of the probes varied with different materials, and some configurations were less effective in quantifying certain components.

Digital Object Identifier (DOI)

10.3390/ph17121659

Want to read the original?

Access the complete publication on the publisher's website

View Original Publication