2-Diazo-1-(1,1-dioxothio­morpholin-4-yl)ethanone
2011

Study of 2-Diazo-1-(1,1-dioxothiomorpholin-4-yl)ethanone

publication Evidence: moderate

Author Information

Author(s): Kaupang Åsmund, Görbitz Carl Henrik, Hansen Tore

Primary Institution: Department of Chemistry, University of Oslo

Conclusion

The crystal structure of the compound shows it predominantly in a chair conformation with some in a boat conformation.

Supporting Evidence

  • The compound was synthesized from a bromo compound using a modified procedure.
  • The crystal structure was determined at a low temperature of 105 K.
  • Five intermolecular interactions were identified in the crystal structure.

Takeaway

The researchers looked at a chemical compound and found that it mostly takes a certain shape, but a tiny bit of it takes a different shape.

Methodology

The compound was synthesized and its crystal structure was analyzed using X-ray diffraction.

Digital Object Identifier (DOI)

10.1107/S1600536811023774

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