Study of a Nickel(II) Complex with a Schiff Base
Author Information
Author(s): Suleiman Gwaram Nura, Saharin Siti Munirah, Khaledi Hamid, Mohd Ali Hapipah
Primary Institution: Department of Chemistry, University of Malaya, Kuala Lumpur, Malaysia
Hypothesis
The study investigates the structure and properties of a nickel(II) complex formed with a Schiff base and thiocyanate ions.
Conclusion
The nickel(II) complex exhibits a unique three-dimensional structure stabilized by hydrogen bonds and C—H⋯π interactions.
Supporting Evidence
- The nickel(II) ion is coordinated by a tridentate Schiff base and two thiocyanate ions.
- The structure features hydrogen bonds that create layers in the crystal.
- The compound was obtained through a reflux process followed by slow evaporation.
Takeaway
The researchers created a special nickel compound that has a unique shape and is held together by tiny connections called bonds.
Methodology
The compound was synthesized by refluxing a mixture of 2-acetylpyridine, N,N-dimethylethyldiamine, nickel(II) acetate tetrahydrate, and sodium thiocyanate in ethanol.
Digital Object Identifier (DOI)
Want to read the original?
Access the complete publication on the publisher's website