Dichloridobis{N,N-diethyl-4-[(pyridin-2-yl-κN)diazen­yl]aniline}zinc [ZnCl2(C15H18N4)2]
2011

Synthesis and Structure of a Zinc Complex with Azoimine Ligand

publication Evidence: moderate

Author Information

Author(s): Leesakul Nararak, Pakawatchai Chaveng, Saithong Saowanit, Tantirungrotechai Yuthana, Kwanplod Kwanchanok

Primary Institution: Prince of Songkla University

Hypothesis

The study investigates the coordination of a zinc ion with a specific azoimine ligand.

Conclusion

The zinc complex exhibits a distorted tetrahedral geometry with specific bond lengths and angles.

Supporting Evidence

  • The zinc ion is coordinated by two nitrogen atoms from the ligand and two chloride ions.
  • The complex shows weak intermolecular hydrogen bonds and π–π interactions.
  • The bond distances in the complex are compared to related compounds.

Takeaway

The researchers made a new zinc compound using a special chemical and found that it has a unique shape.

Methodology

The compound was synthesized by refluxing a solution of the ligand and zinc chloride, followed by crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811022884

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