Metal-Organic Papers(Benzene­carbothio­amide-κS)­penta­carbonyl­tungsten(0) [W(C7H7NS)(CO)5]
2011

Crystal Structure of a Tungsten Complex with Benzene­carbothio­amide

publication Evidence: moderate

Author Information

Author(s): Merniz Salah, Mokhtari Mahiedine, Bouacida Sofiane, Ouahab Lahcène, Mousser Abdelhamid

Primary Institution: Université Mentouri Constantine

Hypothesis

The study aims to synthesize and characterize a new tungsten complex with benzene­carbothio­amide as a ligand.

Conclusion

The crystal structure of the tungsten complex shows a distorted octahedral geometry with five CO groups and a benzene­carbothio­amide ligand.

Supporting Evidence

  • The tungsten atom in the complex is coordinated by five CO groups.
  • The structure exhibits a distorted octahedral geometry.
  • Intermolecular hydrogen bonds link the components into dimeric chains.

Takeaway

Scientists made a new compound using tungsten and a special molecule, and they found out how it is structured.

Methodology

The compound was synthesized by reacting W(CO)6 with benzene­carbothio­amide in dry THF and characterized using X-ray crystallography.

Digital Object Identifier (DOI)

10.1107/S1600536811008579

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