Automatic flow system for simultaneous determination of iron and chromium in steel alloys employing photometers based on LEDs as radiation source
2003

Automatic Flow System for Measuring Iron and Chromium in Steel Alloys

publication Evidence: moderate

Author Information

Author(s): Ridvan N. Fernandes, Boaventura F. Reis, Luis Fernando P. Campos

Primary Institution: Universidade Federal do Maranhao, Brazil

Hypothesis

Can a multicommutated flow system effectively determine iron and chromium in steel alloys using photometry?

Conclusion

The developed flow system accurately measures iron and chromium in steel alloys with low reagent consumption and high throughput.

Supporting Evidence

  • The system achieved an analytical throughput of 160 determinations per hour.
  • Relative standard deviations were 0.4% for iron and 1.2% for chromium.
  • No significant difference was observed when comparing results with ICP-AES.
  • Low reagent consumption was noted, with 0.33 mg for iron and 0.03 mg for chromium per determination.

Takeaway

This study created a machine that can quickly and accurately measure two metals in steel without wasting much material.

Methodology

The study used a microcomputer-controlled flow system with LEDs and photodiodes to measure iron and chromium concentrations in steel alloys.

Limitations

The study may be limited by the specific conditions under which the flow system was tested.

Statistical Information

Confidence Interval

95%

Statistical Significance

p<0.05

Digital Object Identifier (DOI)

10.1080/14639240210166401

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