Metal-Organic Papers(Methanol-κO)(methanolato-κO)oxido[N-(2-oxidobenzylidene)phenylalaninato-κ3 O,N,O′]vanadium(V) [V(C16H13NO3)(CH3O)O(CH4O)]
2011
Synthesis and Structure of a Vanadium Complex
publication
Evidence: moderate
Author Information
Author(s): Bian Lin, Li Lianzhi
Primary Institution: Liaocheng University, Shandong, People's Republic of China
Hypothesis
The study investigates the synthesis and crystal structure of an oxovanadium(V) complex with a tetradentate Schiff-base ligand.
Conclusion
The synthesized vanadium complex exhibits a distorted octahedral coordination geometry.
Supporting Evidence
- The vanadium complex was characterized by X-ray diffraction.
- The coordination involves a tridentate ligand and three oxygen atoms.
- The complex forms a two-dimensional structure due to hydrogen bonding.
Takeaway
Scientists made a special vanadium compound and found that it has a unique shape that helps it hold onto other molecules.
Methodology
The compound was synthesized by mixing L-phenylalanine, potassium hydroxide, and salicylaldehyde in methanol, followed by the addition of vanadyl sulfate.
Digital Object Identifier (DOI)
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