2-Chloro-N-(4-nitro­benzo­yl)benzene­sulfonamide C13H9ClN2O5S
2011

Structure of 2-Chloro-N-(4-nitro­benzo­yl)benzene­sulfonamide

publication Evidence: moderate

Author Information

Author(s): Suchetan P. A., Foro Sabine, Gowda B. Thimme

Primary Institution: Mangalore University

Hypothesis

The study investigates the effect of substituents on the structures of N-(aryl)-amides.

Conclusion

The structure of 2-chloro-N-(4-nitrobenzoyl)-benzenesulfonamide has been determined, revealing specific torsional angles and hydrogen bonding interactions.

Supporting Evidence

  • The N—H bond is anti to the C=O bond, similar to other compounds studied.
  • The dihedral angles between the aromatic rings were measured and compared to previous studies.
  • Molecules are linked into zigzag chains through hydrogen bonds.

Takeaway

The researchers looked at how different chemical groups affect the shape of a specific compound, and they found some interesting angles and connections between the atoms.

Methodology

The compound was synthesized through refluxing a mixture of 4-nitrobenzoic acid, 2-chlorobenzenesulfonamide, and phosphorous oxychloride, followed by crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811009913

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