Organic Papers
2011

Study of Bis(4-ethoxyphenyl) sulfoxide

publication Evidence: moderate

Author Information

Author(s): Meng Kang, Wu Cheng, Cao Jing, Ma Ping, Liu Lihong

Primary Institution: Pharmacy Department of the Second Artillery General Hospital, Beijing, People’s Republic of China

Hypothesis

The study investigates the structure of Bis(4-ethoxyphenyl) sulfoxide prepared via Friedel-Crafts acylation.

Conclusion

The crystal structure of the compound shows a dihedral angle of 82.7° between the benzene rings and features disordered oxygen in the sulfoxide group.

Supporting Evidence

  • The dihedral angle between the benzene rings is 82.7°.
  • The oxygen atom of the sulfoxide group is disordered over two orientations.
  • Molecules are linked by intermolecular C—H⋯O hydrogen bonds.

Takeaway

The researchers made a new chemical compound and looked at its structure using X-ray techniques to see how its parts fit together.

Methodology

The compound was synthesized using Friedel-Crafts acylation and characterized by X-ray diffraction.

Digital Object Identifier (DOI)

10.1107/S1600536811013213

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