Potassium N-bromo-2-chloro­benzene­sulfonamidate sesquihydrate
2011

Structure of Potassium N-bromo-2-chlorobenzenesulfonamidate Sesquihydrate

publication Evidence: moderate

Author Information

Author(s): Gowda B. Thimme, Foro Sabine, Shakuntala K.

Primary Institution: Mangalore University

Hypothesis

To explore the effect of replacing sodium by potassium on the solid state structures of N-haloarylsulfonamidates.

Conclusion

The structure of potassium N-bromo-2-chlorobenzenesulfonamidate sesquihydrate shows hepta-coordination of the K+ ion, differing from the sodium counterpart.

Supporting Evidence

  • The K+ ion is hepta-coordinated by three O atoms from water molecules and four sulfonyl O atoms.
  • The S—N distance of 1.582 Å indicates an S=N double bond.
  • The crystal structure is stabilized by intermolecular hydrogen bonds.

Takeaway

This study looks at how changing sodium to potassium affects the structure of a specific chemical compound.

Methodology

The compound was prepared using a literature method and characterized through X-ray diffraction and spectroscopy.

Digital Object Identifier (DOI)

10.1107/S1600536811022136

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