N′-(5-Chloro-2-oxidobenzyl-κO)-2,4-dihydroxybenzohydrazidato-κ2N′,O](methanol-κO)dioxidomolybdenum(VI)–4,4′-bipyridine (1/1) [Mo(C14H9ClN2O4)O2(CH4O)]·C10H8N2
2011

New Metal-Organic Compound with Schiff Base

publication Evidence: moderate

Author Information

Author(s): Ngan Ngui Khiong, Wong Richard Chee Seng, Lo Kong Mun, Ng Seik Weng

Primary Institution: University of Malaya

Conclusion

The study presents a new co-crystal structure involving a Schiff base and dioxomolybdenum(VI) that forms hydrogen bonds leading to a helical chain.

Supporting Evidence

  • The new compound features a Schiff base that coordinates with a molybdenum atom.
  • Hydrogen bonds in the structure create a helical chain along the b-axis.
  • The study utilized advanced crystallographic techniques to determine the structure.

Takeaway

Scientists created a new compound using a special chemical that helps metals bond in a unique way, forming a spiral structure.

Methodology

The compound was synthesized by condensing 3-ethoxysalicylaldehyde with 2,4-dihydroxybenzohydrazide in methanol, followed by the addition of dioxomolybdenum(VI) and 4,4'-bipyridine.

Digital Object Identifier (DOI)

10.1107/S1600536811017259

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