Determination of Diethyl Phthalate and Polyhexamethylene Guanidine in Surrogate Alcohol from Russia
2011

Detecting Harmful Chemicals in Alcoholic Beverages

Sample size: 22 publication Evidence: moderate

Author Information

Author(s): Yulia B. Monakhova, Thomas Kuballa, Jenny Leitz, Dirk W. Lachenmeier

Primary Institution: Chemisches und Veterinäruntersuchungsamt (CVUA) Karlsruhe

Hypothesis

Can UV-VIS and NMR spectroscopy effectively identify diethyl phthalate (DEP) and polyhexamethylene guanidine (PHMG) in surrogate alcohols?

Conclusion

The study successfully developed and validated UV-VIS and NMR methods for detecting DEP and PHMG in alcoholic beverages.

Supporting Evidence

  • Two out of 22 analyzed alcohol samples contained DEP or PHMG.
  • 1H NMR analysis confirmed the presence of DEP and PHMG in the samples.
  • UV-VIS methods were found to be simple and cost-effective for screening.

Takeaway

Researchers found ways to quickly check if harmful chemicals are in some alcoholic drinks, which can help keep people safe.

Methodology

The study used UV-VIS and 1H NMR spectroscopy to analyze 22 alcohol samples for the presence of DEP and PHMG.

Limitations

The lack of commercial availability of pure PHMG standards limited the quantification methods.

Participant Demographics

Samples included commercial vodkas, medicinal alcohol, homemade samogon, and surrogate alcohol from three cities in Russia.

Statistical Information

Statistical Significance

p<0.05

Digital Object Identifier (DOI)

10.1155/2011/704795

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