2-Methyl-N-(4-nitro­benzo­yl)benzene­sulfonamide
2011

Structure of 2-Methyl-N-(4-nitro­benzo­yl)benzene­sulfonamide

publication Evidence: moderate

Author Information

Author(s): Suchetan P. A., Foro Sabine, Gowda B. Thimme

Primary Institution: Mangalore University

Hypothesis

The study investigates the effect of substituents on the structures of N-(aryl)-amides.

Conclusion

The conformation of the N—C bond in the compound exhibits gauche torsions with respect to the S=O bonds.

Supporting Evidence

  • The molecule is twisted at the S atom with a specific torsion angle.
  • The dihedral angles between different segments of the molecule were measured.
  • Molecules are linked into zigzag chains via hydrogen bonds.

Takeaway

This study looks at how different parts of a molecule can change its shape, specifically in a compound that has a sulfonamide group.

Methodology

The compound was prepared by refluxing a mixture of 4-nitrobenzoic acid, 2-methylbenzenesulfonamide, and phosphorous oxychloride, followed by crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811009846

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