Hydrazine-1,2-diium bis­(3-carb­oxy-4-hy­droxy­benzene­sulfonate) tetra­hydrate
2011

Hydrated Salt Formation from 5-Sulfosalicylic Acid and Hydrazine

publication Evidence: moderate

Author Information

Author(s): Selvaraju Devipriya, Venkatesh Ranjithkumar, Sundararajan Vairam

Primary Institution: Government College of Technology, Coimbatore, India

Hypothesis

The reaction of 5-sulfosalicylic acid with hydrazine hydrate at pH 1 will yield a specific hydrated salt.

Conclusion

The study successfully synthesized a hydrated salt and characterized its crystal structure, revealing significant hydrogen bonding interactions.

Supporting Evidence

  • The title compound was formed through a reaction at pH 1.
  • The crystal structure was analyzed using single-crystal X-ray diffraction.
  • Significant hydrogen bonding interactions were observed in the crystal structure.

Takeaway

When you mix a strong acid with a special base, they can form a new solid that has a unique structure. This study shows how that happens.

Methodology

The compound was synthesized by dissolving 5-sulfosalicylic acid and hydrazine hydrate in distilled water at pH 1, followed by crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811014231

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