1-[(3-Chloro­phen­yl)(morpholin-4-yl)­meth­yl]naphthalen-2-ol
2011

Synthesis and Crystal Structure of a New Compound

publication Evidence: moderate

Author Information

Author(s): Shu Li-Jin

Primary Institution: Hangzhou Normal University

Conclusion

The study successfully synthesized and characterized the compound 1-[(3-Chlorophenyl)(morpholin-4-yl)methyl]naphthalen-2-ol, revealing its crystal structure.

Supporting Evidence

  • The dihedral angle between the naphthylene ring system and the phenyl ring is 77.86°.
  • The morpholine ring adopts a chair conformation.
  • The hydroxyl group is involved in intramolecular hydrogen bonding.

Takeaway

Scientists made a new chemical compound and looked at its structure using special X-ray techniques to understand how it is built.

Methodology

The compound was synthesized by mixing 3-chlorobenzaldehyde, naphthalen-2-ol, and morpholine in a dry flask, followed by heating and crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811021726

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