The Phospha–Michael addition product {(t-BuNH)P(μ-N-t-Bu)2P(=N-t-Bu)—C(=CH2)CH(p-CH3O—C6H4)-P(O)[(OCH2C(CH3)2CH2O)]} C31H57N4O4P3
2011
Synthesis of a New Phospha–Michael Addition Product
publication
Evidence: moderate
Author Information
Author(s): Gangadhararao G., Venu Srinivas
Primary Institution: University of Hyderabad
Hypothesis
The reaction of cyclodiphosphazane with allenylphosphonate will yield a new compound.
Conclusion
The synthesized compound exhibits a unique crystal structure with specific hydrogen bonding interactions.
Supporting Evidence
- The compound was synthesized with a yield of 92%.
- The crystal structure was determined at 100 K.
- Hydrogen bonds were identified as key interactions in the crystal packing.
Takeaway
Scientists made a new chemical compound by mixing two other chemicals together, and they found that it formed crystals with interesting shapes.
Methodology
The compound was synthesized through a Phospha–Michael addition reaction and characterized using X-ray crystallography.
Limitations
Attempts to solve the structure in a higher symmetry space group were unsuccessful.
Digital Object Identifier (DOI)
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