Diaqua­bis­(2-oxo-2H-chromene-3-carboxyl­ato-κ2O2,O3)manganese(II)
2011

New Manganese Complex with Coumarin

publication Evidence: moderate

Author Information

Author(s): Cui Yue, Gao Qian, Wang Huan-Huan, Wang Lin, Xie Ya-Bo

Primary Institution: Beijing University of Technology

Hypothesis

The study investigates the synthesis and crystal structure of a new manganese complex coordinated by coumarin-3-carboxylic acid.

Conclusion

The manganese(II) complex exhibits a slightly distorted octahedral geometry with specific bond distances and angles.

Supporting Evidence

  • The manganese(II) atom is six-coordinated by two O atoms from water and four O atoms from coumarin ligands.
  • The Mn—O bond distances range from 2.0931 to 2.2315 Å.
  • O—H⋯O hydrogen bonds link the complex molecules into two-dimensional layers.

Takeaway

Scientists made a new manganese compound using a special acid, and they found that it has a unique shape.

Methodology

The complex was synthesized by layering solutions of manganese sulfate, coumarin-3-carboxylic acid, and lithium hydroxide, followed by crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811016667

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