[η5-(Phenyl­ethyn­yl)cyclo­penta­dien­yl](η4-tetra­phenyl­cyclo­butadiene)cobalt(I) [Co(C13H9)(C28H20)]
2011

Structure of a Cobalt Complex with Cyclopentadienyl and Cyclobutadienyl Rings

publication Evidence: high

Author Information

Author(s): Courtney Donagh, Manning Anthony R., McAdam C. John, Simpson Jim

Primary Institution: University College Dublin

Conclusion

The crystal structure of the cobalt complex is stabilized by C—H⋯π interactions, forming a three-dimensional network.

Supporting Evidence

  • The cobalt atom is sandwiched between cyclopentadienyl and cyclobutadienyl rings.
  • The dihedral angle between the rings is 2.6°.
  • The phenyl rings are tilted in a four-bladed propeller configuration.

Takeaway

Scientists studied a cobalt compound that has special rings around it, and they found that these rings help hold the structure together in a unique way.

Methodology

The compound was synthesized using the Castro-Stephens coupling method and characterized using X-ray crystallography.

Digital Object Identifier (DOI)

10.1107/S1600536811016928

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