3,3′-Dinitro-4,4′-bipyridine
2011

Crystal Structure of 3,3'-Dinitro-4,4'-bipyridine

publication Evidence: moderate

Author Information

Author(s): Wang Yong, Xu Jing-Yi, Li De-Yong, Shi Lu

Primary Institution: Henan Polytechnic Institute

Conclusion

The study reports the crystal structure of 3,3'-dinitro-4,4'-bipyridine, revealing its molecular arrangement and interactions.

Supporting Evidence

  • The dihedral angle of the pyridine rings in the compound is 67.8°.
  • Intermolecular C—H⋯O and C—H⋯N interactions link the molecules into a three-dimensional network.
  • The bond lengths and angles in the structure are within normal ranges.

Takeaway

The researchers looked at how the molecules of a compound called 3,3'-dinitro-4,4'-bipyridine are arranged and connected in a crystal.

Methodology

The compound was synthesized using the Ullmann reaction and crystals were obtained by dissolving it in ethanol and evaporating the solvent.

Digital Object Identifier (DOI)

10.1107/S1600536811014139

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