(1S,3R,8R,11S)-2,2-Dichloro-3,7,7,10-tetramethyltricyclo[6.4.0.01,3]dodec-9-en-11-ol
2011
Synthesis and Structure of a New Compound from β-himachalene
publication
Evidence: moderate
Author Information
Author(s): Benharref Ahmed, Lassaba Essêdiya, Avignant Daniel, Oudahmane Abdelghani, Berraho Moha
Primary Institution: Laboratoire de Chimie Biomoléculaires, Substances Naturelles et Réactivité, URAC16, Faculté des Sciences, Semlalia, Marrakech, Morocco
Conclusion
The study successfully synthesized a new compound from β-himachalene and determined its structure through crystallographic analysis.
Supporting Evidence
- The compound was synthesized from β-himachalene, which is derived from the essential oil of the Atlas cedar.
- The structure was confirmed through NMR spectral analysis and mass spectroscopy.
- The crystal structure revealed that molecules aggregate into supramolecular chains mediated by hydrogen bonds.
Takeaway
Scientists made a new chemical from a natural substance and figured out what it looks like using special techniques.
Methodology
The compound was synthesized using a reaction involving dichlorocarbene and N-bromosuccinimide, followed by crystallization.
Digital Object Identifier (DOI)
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