Tris(tetra­butyl­ammonium) tris­(nitrato-κ2 O,O′)tetra­kis­(thio­cyanato-κN)thorium(IV) (C16H36N)3[Th(NCS)4(NO3)3]
2011

Structure of a Thorium Complex

publication Evidence: high

Author Information

Author(s): Lozano-Rodriguez M. Janeth, Thuéry Pierre, Petit Sébastien, Copping Roy, Mustre de Leon Jose, Den Auwer Christophe

Primary Institution: CEA, Nuclear Energy Division, Radio Chemistry and Processes Department, F-30207 Bagnols sur Cèze, France

Conclusion

The study successfully determined the crystal structure of a new thorium complex with specific coordination properties.

Supporting Evidence

  • The compound was obtained from the reaction of Th(NO3)4·5H2O with tetrabutylammonium thiocyanate.
  • The ThIV atom is in a ten-coordinate environment of irregular geometry.
  • The average Th—N and Th—O bond lengths were measured as 2.481 (10) and 2.57 (3) Å, respectively.

Takeaway

Scientists created a new compound with thorium and studied its structure to understand how it is built.

Methodology

The compound was synthesized and characterized using X-ray crystallography.

Digital Object Identifier (DOI)

10.1107/S1600536811009792

Want to read the original?

Access the complete publication on the publisher's website

View Original Publication