Synthesis and Properties of N-Bromosuccinimide Derivatives of Ammonium Dialkyl/Alkylene Dithiophosphates
2007
Synthesis and Properties of N-Bromosuccinimide Derivatives
publication
Evidence: moderate
Author Information
Author(s): Neelam Harkut, Padam N. Nagar
Primary Institution: University of Rajasthan
Hypothesis
The study investigates the reaction of N-bromosuccinimide with ammonium dialkyl/alkylene dithiophosphates to form new derivatives.
Conclusion
The reaction produces reddish-brown sticky liquids that exhibit a P−S−N chemical linkage.
Supporting Evidence
- The reaction proceeds to completion within 6-7 hours.
- The newly synthesized complexes were characterized by IR and NMR spectroscopy.
- The formation of P−S−N chemical linkage was established through spectral evidence.
Takeaway
The researchers mixed a chemical called N-bromosuccinimide with another compound to create new sticky liquids that have special properties.
Methodology
The reaction was carried out in refluxing benzene solution and characterized using physicochemical and spectroscopic techniques.
Limitations
The compounds could not be crystallized for X-ray analysis due to their sticky nature.
Digital Object Identifier (DOI)
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