N-(2-Chloro-2,2-difluoro­acet­yl)-N′,N′′-diisopropyl­phospho­ric triamide
2011

Crystal Structure of a Phosphoric Triamide Compound

publication Evidence: moderate

Author Information

Author(s): Pourayoubi Mehrdad, Saneei Anahid

Primary Institution: Ferdowsi University of Mashhad

Conclusion

The study presents the synthesis and crystal structure of a new phosphoric triamide compound, revealing its unique bonding and structural characteristics.

Supporting Evidence

  • The compound features a phosphoryl group and NH unit in a syn conformation.
  • The phosphorus atom exhibits a slightly distorted tetrahedral configuration.
  • Adjacent molecules in the crystal are linked by hydrogen bonds, forming specific ring structures.

Takeaway

Scientists made a new chemical compound and looked at its structure using special techniques to understand how its atoms are arranged.

Methodology

The compound was synthesized from a reaction involving phosphorus pentachloride and a chlorinated amide, followed by crystallization from a methanol/acetonitrile mixture.

Digital Object Identifier (DOI)

10.1107/S1600536811005435

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