Redetermination of 6,6′-dimeth­oxy-2,2′-[hexane-1,6-diylbis(nitrilo­dimethyl­idyne)]diphenol
2011

Redetermination of a Chemical Compound Structure

publication Evidence: moderate

Author Information

Author(s): Tabatabaee M., Fotuhiardakani M. R., Lough Alan J.

Primary Institution: Department of Chemistry, Yazd Branch, Islamic Azad University, Yazd, Iran

Hypothesis

The study aims to redetermine the crystal structure of 6,6′-dimeth­oxy-2,2′-[hexane-1,6-diylbis(nitrilo­dimethyl­idyne)]diphenol.

Conclusion

The study found that one molecule crystallizes in a neutral form while the other crystallizes in a zwitterionic form.

Supporting Evidence

  • The study identified two independent centrosymmetric molecules in the compound.
  • Significant differences in bond lengths supported the existence of zwitterionic and neutral forms.
  • Intermolecular hydrogen bonds were observed forming one-dimensional chains in the crystal.

Takeaway

The researchers looked at a chemical compound and found that it can exist in two different forms, one neutral and one charged.

Methodology

The crystal structure was determined using X-ray diffraction techniques.

Digital Object Identifier (DOI)

10.1107/S1600536811020599

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