N,N′-Di­benzyl­ethyl­enedi­ammonium dichloride
2024

Study of N,N′-Di­benzyl­ethyl­enedi­ammonium dichloride

publication Evidence: moderate

Author Information

Author(s): Marmande Mary Helene, Baxter Bailey N., Zeller Matthias, Forbes David C.

Primary Institution: University of South Alabama

Hypothesis

The study investigates the unexpected formation of N,N′-di­benzyl­ethyl­enedi­ammonium dichloride during a synthetic organic chemistry course.

Conclusion

The study confirms the importance of conducting undergraduate research where outcomes are not predetermined, highlighting the unexpected formation of a new compound.

Supporting Evidence

  • The unexpected product was identified through single crystal X-ray diffraction.
  • The study emphasizes the value of undergraduate research experiences.
  • Strong hydrogen bonds were found in the solid-state structure of the compound.

Takeaway

This study shows that sometimes experiments can lead to surprising results, like creating a new chemical compound instead of the one we expected.

Methodology

The compound was synthesized through a reaction involving benzyl­amine and 1,2-di­chloro­ethane, followed by crystallization and analysis using single crystal X-ray diffraction.

Limitations

The study does not report on the reproducibility of the unexpected product formation or the potential for other side reactions.

Participant Demographics

Undergraduate students participating in a course-based research experience.

Digital Object Identifier (DOI)

10.1107/S205698902400954X

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