Tris(1,10-phenanthroline)cadmium 3,3′-dicarb­oxy-4,4′-diazenedi­yl­dibenzoate–4,4′-diazenediyldiphthalic acid–methanol (1/0.5/1)
2011

Structure of a Cadmium Complex with Phenanthroline and Dicarboxylic Acid

publication Evidence: moderate

Author Information

Author(s): Wang Jun, Lu Lu, Wei-Ping Wu, He Xi-Yang, Tao Wang

Primary Institution: Sichuan University of Science and Engineering

Hypothesis

The study investigates the self-assembly of Cd(II) ions with specific ligands to form a complex.

Conclusion

The cadmium complex exhibits a distorted octahedral coordination with unique hydrogen bonding interactions.

Supporting Evidence

  • The cadmium atom is coordinated by six nitrogen atoms from three phenanthroline ligands.
  • The structure features both deprotonated and undeprotonated dicarboxylic acid molecules.
  • Hydrogen bonds link the deprotonated and undeprotonated molecules, forming a one-dimensional chain.

Takeaway

The researchers created a new compound using cadmium and certain organic molecules, which formed a special structure with interesting properties.

Methodology

The compound was synthesized by mixing cadmium acetate with ligands in methanol and allowing it to react at room temperature for 15 days.

Limitations

The disordered methanol molecules in the structure were not fully modeled.

Digital Object Identifier (DOI)

10.1107/S160053681102068X

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