Poly[di-μ2-aqua-μ2-(5-methyl­pyrazine-2-carboxyl­ato)-(5-methyl­pyrazine-2-carboxyl­ato)-μ3-nitrato-trilithium] [Li3(C6H5N2O2)2(NO3)(H2O)2]
2011

Structure of a Lithium Complex with 5-Methylpyrazine-2-Carboxylate

publication Evidence: high

Author Information

Author(s): Wojciech Starosta, Janusz Leciejewicz

Primary Institution: Institute of Nuclear Chemistry and Technology, Warsaw, Poland

Conclusion

The study presents the crystal structure of a lithium complex that features a unique arrangement of lithium ions and organic ligands.

Supporting Evidence

  • The asymmetric unit contains three lithium ions, two ligand anions, two water molecules, and a nitrate anion.
  • The coordination environment of the lithium ions includes various oxygen and nitrogen atoms from the ligands.
  • The structure features molecular columns held together by hydrogen bonds and π–π interactions.

Takeaway

Scientists studied a special compound made of lithium and a type of organic molecule, and they found out how these parts fit together in a crystal.

Methodology

The compound was synthesized by mixing hot aqueous solutions of 5-methylpyrazine-2-carboxylic acid and lithium nitrate, followed by crystallization.

Digital Object Identifier (DOI)

10.1107/S1600536811024548

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