2-(4-Methoxyphenyl)-4H-1,3,2-benzoxathiaphosphinine 2-sulfide
2011
Study of a New Compound: 2-(4-Methoxyphenyl)-4H-1,3,2-benzoxathiaphosphinine 2-sulfide
publication
Evidence: moderate
Author Information
Author(s): Osyanin Vitaly A., Ivleva Elena A., Rybakov Victor B., Klimochkin Yurij N.
Primary Institution: Samara State Technical University
Conclusion
The study successfully synthesized a new compound with specific structural characteristics.
Supporting Evidence
- The compound was synthesized from Lawesson's reagent and o-hydroxybenzyl alcohol.
- X-ray analysis revealed two independent molecules with different conformations.
- Weak interactions were observed between sulfur atoms and hydrogen atoms in the crystal structure.
Takeaway
Researchers created a new chemical compound and studied its structure using X-ray analysis.
Methodology
The compound was synthesized using Lawesson's reagent and characterized by X-ray diffraction, NMR, and IR spectroscopy.
Limitations
Technical problems during the diffraction experiment led to the loss of 87 reflections.
Digital Object Identifier (DOI)
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